Ethers and Their Oligomeric Derivatives Obtained from 2,4,6,8-Tetra(hydroxymethyl)glycoluril

Svetlana Yu. Panshina, О. V. Ponomarenko, А. А. Бакибаев, Victor S. Malkov, A. A. Zhortarova

2023

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DOI 10.1134/s1070363223150069
Data confidence 70 medium
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Abstract

Abstract In this work, a series of 2,4,6,8-tetra(alkoxymethyl)glycoluril esters and their derivatives was synthesized for the first time, starting from 2,4,6,8-tetra(hydroxymethyl)glycoluril, the properties and spectral data of the synthesized compounds were described. Individual oligomers, derivatives of 2,4,6,8-tetra(methoxymethyl)glycoluril, were isolated and identified, their structures were described using HPLC analysis and IR and NMR spectroscopy. A similar possibility for the dimerization/oligomerization reactions of 2,4,6,8-tetra(ethoxymethyl)-, 2,4,6,8-tetra(isopropoxymethyl)-, and 2,4,6,8-tetra(butoxymethyl) derivatives of glycoluril with the release of macrocomponents was shown.