Synthesis and structure of N-methyl-1-[(4-bromo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]fullerene-C60-[1,9-c]pyrrolidine

Serik D. Fazylov, О. А. Нуркенов, А. Е. Аринова, Т. М. Сейлханов, Airat R. Tuktarov, Artur A. Khuzin, Ryszhan Y. Bakirova, Л. Е. Муравлева

2015

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DOI 10.1134/s1070363215050072

Data confidence 70 medium

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Abstract

Three-component condensation of fullerene C 60 with sarcosine and 4-(4-bromo-3,5-dimethyl-1 H -pyrazol-1-yl)benzaldehyde under the conditions of the Prato reaction has afforded new fulleropyrrolidine; the product structure has been confirmed by IR and NMR spectroscopy as well as mass spectrometry.