Response Surface Optimization of Apple Powder Incorporation and Processing Conditions for Improving the Quality of Whipped Yeast-Free Frozen Dough and Bread

Sholpan Tursunbayeva, Аuyelbek Iztayev, Zhuldyz Nurgozhina, Madina Asatullaevna Yakiyayeva, Bauyrzhan Iztayev, Bayan Zh. Muldabekova, М.Н. Мамыраев, Diana Bayshagylovna Abdraimova, Fatima Yermetaeva

2026

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DOI 10.3390/pr14152500
Data confidence 70 medium
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Abstract

Mechanically aerated yeast-free dough is particularly susceptible to freeze–thaw damage because its porous structure is formed before freezing and cannot be restored during thawing due to the absence of fermentation. This study investigated the combined effects of apple powder incorporation and technological processing conditions on the rheological, structural, physicochemical, nutritional, and sensory properties of whipped yeast-free frozen dough and the resulting bread. Apple powder was incorporated at three formulation levels (50, 100, and 150 g per batch), while whipping speed (450–900 rpm), whipping time (3–7 min), freezing temperature (−14 to −38 °C), and microwave thawing time (4–8 min) were optimized using response surface methodology based on a Draper–Lin composite design. Dough properties were evaluated using Mixolab analysis and structural–mechanical measurements, whereas bread quality was assessed by specific volume, porosity, physicochemical characteristics, biochemical composition, amino acid profile, microbiological safety, and sensory evaluation. The developed regression models adequately described the effects of technological variables on dough quality (R2 > 0.95). Deep freezing at −38 °C followed by 4 min of microwave thawing minimized structural deterioration and improved dough stability after freeze–thaw treatment. Apple powder increased the nutritional value of the bread by enhancing the dietary fiber (4.8–7.3%), potassium (125.6–156.7 mg/100 g), iron (2.45–3.20 mg/100 g), and vitamin C (0–2.2 mg/100 g) contents. Although the highest level of apple powder provided the greatest nutritional enrichment, it also reduced the dough rheological stability and produced a less homogeneous crumb structure. Overall, the formulation containing 100 g of apple powder per batch combined with a whipping speed of 900 rpm, whipping time of 7 min, freezing at −38 °C, and microwave thawing for 4 min provided the best balance between rheological stability, freeze–thaw resistance, bread quality, nutritional enhancement, microbiological stability, and sensory acceptability. These findings demonstrate that simultaneous optimization of formulation and processing conditions is an effective strategy for improving mechanically aerated yeast-free frozen bakery products and provides a scientific basis for the development of functional frozen bread technologies.