Abstract
The present study investigates the development of non-autoclaved aerated concrete (NAAC) incorporating rice husk ash (RHA)-derived amorphous silica, polypropylene microfibers, and a polycarboxylate-based superplasticizer to improve mechanical performance and durability while maintaining low density and thermal conductivity. Experimental investigations included density, compressive strength, thermal conductivity, water absorption, X-ray diffraction (XRD), microstructural observations, and TG–DTA analysis. The developed compositions containing 5–7% RHA and 0.10–0.20% polypropylene microfibers achieved compressive strength values of 4.5–4.8 MPa at densities of 520–560 kg/m3, which are comparable to or higher than values commonly reported for non-autoclaved aerated concrete of similar density. Thermal conductivity decreased to 0.12–0.13 W/(m·K), while water absorption was reduced to 15–18%. XRD, microstructural, and TG–DTA analyses suggested enhanced hydration reactions and improved development of the cementitious matrix due to pozzolanic interaction between amorphous silica and calcium hydroxide. The incorporation of polypropylene microfibers was associated with improved structural homogeneity of the developed NAAC compositions, whereas the superplasticizer enhanced mixture homogeneity and pore stability. The results suggest that the combined use of agricultural waste-derived silica and fiber reinforcement provides an effective approach for producing sustainable and energy-efficient NAAC without autoclave curing.