Изготовление эффективного электродного материала для химических накопителей энергии из чайной биомассы методом микроволновой карбонизации и физической активации

2025

Full text Open access: Hybrid Metadata (CSL-JSON)
DOI 10.18321/cpc23(2)185-192
Data confidence 70 medium
How this score is calculated

It is built from checkable properties of the record itself: whether the article has a DOI, how many independent sources confirmed its data, whether the required fields are filled in, and how recent the latest confirmation is. Disagreement between sources and a missing identifier lower it. A value of 80 or above means the record was published without further checking; 60 to 79 means it is published at reduced confidence, with a manual check advisable. A record verified by an editor by hand is never pushed below 90 by a recalculation. This scores our data about the article, not the article itself.

Abstract

This work is intended to study and use carbon material obtained from tea leaf waste in energy storage systems. Microwave carbonization accompanied by physical activation in a CO2 atmosphere was used as a synthesis method. Silicon carbide was used to increase the heating efficiency to ensure uniform heat distribution in the reaction zone. The obtained activated carbon is characterized by a porous structure and good electrical conductivity. The structural and morphological properties of the samples were studied by X-ray diffraction analysis, scanning electron microscopy and Raman spectroscopy. The electrochemical characteristics were evaluated by cyclic voltammetry, galvanostatic charge-discharge and electrochemical impedance spectroscopy. The ФА-30 sample showed high specific capacitance (up to 152 F/g) and high stability during long-term cycling - after 3000 cycles it retained more than 75% of the initial capacity. Electrochemical impedance spectroscopy analysis showed that the porous structure of the material has a low series resistance of about 1 Ohm and a very low charge transfer resistance, which indicates good ion conductivity and fast electrochemical processes. The results obtained prove that the prepared material is promising for use in supercapacitor electrodes.