Аннотация
Silver chloride nanoparticles prepared by exchange mechanochemical reaction NH 4 Cl + AgNO 3 + z NH 4 NO 3 = ( z + 1)NH 4 NO 3 + AgCl in ammonium nitrate matrix (diluent and side reaction product) at dilution parameters z = 7.22 and 3.64 are studied by X-ray diffraction and thermal analysis, electron microscopy, and dynamic light scattering. It is shown that free-form AgCl nanoparticles can be obtained after removal of ammonium nitrate by washing-out with water or thermal annealing at 300°C.